Philip A Smith

Summary

Affiliation: Uniformed Services University of the Health Sciences
Country: USA

Publications

  1. ncbi request reprint Gas chromatography using a resistively heated column with mass spectrometric detection for rapid analysis of pyridine released from Bacillus spores
    Philip A Smith
    Department of Preventive Medicine and Biometrics, Uniformed Services University of the Health Sciences, 4301 Jones Bridge Road, Bethesda, MD 20814, USA
    J Chromatogr A 1036:249-53. 2004
  2. doi request reprint Artifacts related to N-methyl-N-(tert-butyldimethylsilyl)trifluoroacetamide derivatization of citrulline revealed by gas chromatography-mass spectrometry using both electron and chemical ionization
    Philip A Smith
    Department of Preventive Medicine and Biometrics, Uniformed Services University of the Health Sciences, Bethesda, MD 20814 4712, USA
    J Chromatogr A 1217:5444-8. 2010
  3. ncbi request reprint Formation of 2-chlorobenzylidenemalononitrile (CS riot control agent) thermal degradation products at elevated temperatures
    Timothy A Kluchinsky
    Department of Preventive Medicine and Biometrics, Uniformed Services University of the Health Sciences, Bethesda, MD 20814 4799, USA
    J Chromatogr A 952:205-13. 2002
  4. ncbi request reprint Traditional sampling with laboratory analysis and solid phase microextraction sampling with field gas chromatography/mass spectrometry by military industrial hygienists
    Philip A Smith
    Uniformed Services University of the Health Sciences, Department of Preventive Medicine and Biometrics, Bethesda, MD, USA
    AIHA J (Fairfax, Va) 63:284-92. 2002
  5. ncbi request reprint Application of headspace solid-phase microextraction and gas chromatography-mass spectrometry for detection of the chemical warfare agent bis(2-chloroethyl) sulfide in soil
    Gregory L Kimm
    Uniformed Services University of the Health Sciences, Department of Preventive Medicine and Biometrics, Bethesda, MD 20814, USA
    J Chromatogr A 971:185-91. 2002
  6. ncbi request reprint Volatile organic compounds produced during irradiation of mail
    Philip A Smith
    Department of Preventive Medicine and Biometrics, Uniformed Services University of the Health Sciences, 4301 Jones Bridge Road, Bethesda, MD 20814 4799, USA
    AIHA J (Fairfax, Va) 64:189-95. 2003
  7. ncbi request reprint Detection of VX contamination in soil through solid-phase microextraction sampling and gas chromatography/mass spectrometry of the VX degradation product bis(diisopropylaminoethyl)disulfide
    Gary L Hook
    Uniformed Services University of the Health Sciences, Department of Preventive Medicine and Biometrics, Bethesda, MD 20814 4799, USA
    J Chromatogr A 992:1-9. 2003
  8. ncbi request reprint Dynamic solid phase microextraction for sampling of airborne sarin with gas chromatography-mass spectrometry for rapid field detection and quantification
    Gary L Hook
    Uniformed Services University of the Health Sciences, Department of Preventive Medicine and Biometrics, Bethesda MD, USA
    J Sep Sci 27:1017-22. 2004

Collaborators

  • Gary L Hook
  • Paul B Savage
  • Gregory L Kimm
  • Timothy A Kluchinsky
  • Carmela Jackson Lepage
  • Stephen I Miller
  • Gregory Kimm
  • Bangwei Ding
  • David Koch
  • Michael V Sheely

Detail Information

Publications8

  1. ncbi request reprint Gas chromatography using a resistively heated column with mass spectrometric detection for rapid analysis of pyridine released from Bacillus spores
    Philip A Smith
    Department of Preventive Medicine and Biometrics, Uniformed Services University of the Health Sciences, 4301 Jones Bridge Road, Bethesda, MD 20814, USA
    J Chromatogr A 1036:249-53. 2004
    ..Throughput of 20 analyses per hour was shown to be possible with a 1-min column cool-down time between analyses...
  2. doi request reprint Artifacts related to N-methyl-N-(tert-butyldimethylsilyl)trifluoroacetamide derivatization of citrulline revealed by gas chromatography-mass spectrometry using both electron and chemical ionization
    Philip A Smith
    Department of Preventive Medicine and Biometrics, Uniformed Services University of the Health Sciences, Bethesda, MD 20814 4712, USA
    J Chromatogr A 1217:5444-8. 2010
    ..Linear-programmed temperature GC retention index data relative to n-alkanes are reported for observed GC peaks...
  3. ncbi request reprint Formation of 2-chlorobenzylidenemalononitrile (CS riot control agent) thermal degradation products at elevated temperatures
    Timothy A Kluchinsky
    Department of Preventive Medicine and Biometrics, Uniformed Services University of the Health Sciences, Bethesda, MD 20814 4799, USA
    J Chromatogr A 952:205-13. 2002
    ..We conclude that the production of many CS-derived compounds previously observed during high-temperature dispersion is likely to be heat related...
  4. ncbi request reprint Traditional sampling with laboratory analysis and solid phase microextraction sampling with field gas chromatography/mass spectrometry by military industrial hygienists
    Philip A Smith
    Uniformed Services University of the Health Sciences, Department of Preventive Medicine and Biometrics, Bethesda, MD, USA
    AIHA J (Fairfax, Va) 63:284-92. 2002
    ..Both sampling/analysis methods were used to detect CS riot control agent-derived air contaminants dispersed from riot control type canisters through oxidizer-supported combustion of a chemical fuel...
  5. ncbi request reprint Application of headspace solid-phase microextraction and gas chromatography-mass spectrometry for detection of the chemical warfare agent bis(2-chloroethyl) sulfide in soil
    Gregory L Kimm
    Uniformed Services University of the Health Sciences, Department of Preventive Medicine and Biometrics, Bethesda, MD 20814, USA
    J Chromatogr A 971:185-91. 2002
    ..As completed here, total time for sampling and analysis was just under 1 h, and use of organic solvents or special sample introduction equipment was avoided...
  6. ncbi request reprint Volatile organic compounds produced during irradiation of mail
    Philip A Smith
    Department of Preventive Medicine and Biometrics, Uniformed Services University of the Health Sciences, 4301 Jones Bridge Road, Bethesda, MD 20814 4799, USA
    AIHA J (Fairfax, Va) 64:189-95. 2003
    ..These similarities should guide additional work to examine irradiated mail for chemical compounds not detectable by methods used here...
  7. ncbi request reprint Detection of VX contamination in soil through solid-phase microextraction sampling and gas chromatography/mass spectrometry of the VX degradation product bis(diisopropylaminoethyl)disulfide
    Gary L Hook
    Uniformed Services University of the Health Sciences, Department of Preventive Medicine and Biometrics, Bethesda, MD 20814 4799, USA
    J Chromatogr A 992:1-9. 2003
    ..This method is relatively rapid (less than 1 h), avoids the use of complex preparation steps, and enhances analyst safety through limited use of solvents and decontamination of the soil before sampling...
  8. ncbi request reprint Dynamic solid phase microextraction for sampling of airborne sarin with gas chromatography-mass spectrometry for rapid field detection and quantification
    Gary L Hook
    Uniformed Services University of the Health Sciences, Department of Preventive Medicine and Biometrics, Bethesda MD, USA
    J Sep Sci 27:1017-22. 2004
    ....