Research Topics
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Publications
Spectrophotometric method for the determination of nifedipine with 4-(methylamino)phenol and potassium dichromateNafisur Rahman
Department of Chemistry, Aligarh Muslim University, India
Farmaco 57:435-41. 2002..9 x 10(3) l mol(-1) cm(-1), 1.1 microg ml(-1), 99.7-100.5% and 0.3-0.8%, respectively. The proposed method was compared favourably with the official B.P. method...
Kinetic spectrophotometric method for the determination of ramipril in pharmaceutical formulationsNafisur Rahman
Department of Chemistry, Aligarh Muslim University, Aligarh 202002, Uttar Pradesh, India
AAPS PharmSciTech 6:E543-51. 2005..The experimental true bias of all samples is less than +/- 2%. The methods have been successfully applied to the determination of ramipril in tablets and capsules...
Quantitative analysis of irbesartan in commercial dosage forms by kinetic spectrophotometryNafisur Rahman
Department of Chemistry, Aligarh Muslim University, Aligarh 202002, Uttar Pradesh, India
Chem Pharm Bull (Tokyo) 54:626-31. 2006..The methods have been successfully applied to the determination of irbesartan in commercial dosage forms...
Kinetic spectrophotometric analysis of pantoprazole in commercial dosage formsNafisur Rahman
Department of Chemistry, Aligarh Muslim University, Aligarh 202002, Uttar Predesh, India
Anal Sci 22:983-8. 2006..The experimental true bias of all samples is < +/-2.0%. The method has been successfully applied to the determination of pantoprazole in pharmaceutical preparations...
Quantitation of nicorandil in pharmaceutical formulations by spectrophotometry using N-(1-naphthyl) ethylenediamine dihydrochloride as coupling agentNafisur Rahman
Department of Chemistry, Aligarh Muslim University, Uttar Pradesh, India
Yakugaku Zasshi 127:367-74. 2007....
Selective and validated spectrophotometric methods for the determination of nicorandil in pharmaceutical formulationsNafisur Rahman
Department of Chemistry, Aligarh Muslim University, Aligarh 202002, Uttar Pradesh, India
AAPS J 6:e34. 2004..The reliability and the performance of the proposed methods are established by point and interval hypothesis and through recovery studies. The experimental true bias of all samples is smaller than +/-2%...
Validated spectrophotometric methods for the determination of amiodarone hydrochloride in commercial dosage forms using p-chloranilic acid and 2,3-dichloro-5,6-dicyano-1,4-benzoquinoneNafisur Rahman
Department of Chemistry, Aligarh Muslim University, Aligarh 202002 UP, India
Anal Sci 20:1231-5. 2004..Beer's law is obeyed in the concentration ranges 10.0 - 360.0 and 2.0 - 65.0 microg ml(-1) for methods A and B, respectively. Application of the proposed methods to commercial pharmaceutical tablets are presented...
Spectrophotometric method for the determination of verapamil hydrochloride in pharmaceutical formulations using N-bromosuccinimide as oxidantNafisur Rahman
Department of Chemistry, Aligarh Muslim University, Aligarh 202002, UP, India
Farmaco 59:529-36. 2004..Results of analyses were optimized and validated statistically and through recovery studies. The experimental true bias of all samples is smaller than +/-2%...
Optimized and validated spectrophotometric methods for the determination of nicorandil in drug formulations and biological fluidsNafisur Rahman
Department of Chemistry, Aligarh Muslim University, Aligarh 202002, UP, India
Farmaco 59:519-27. 2004..In order to establish the bias and the performance of the proposed methods, the point and interval hypothesis tests have been performed. The experimental true bias of all samples is smaller than +/-2%...
Kinetic spectrophotometric method for the determination of silymarin in pharmaceutical formulations using potassium permanganate as oxidantN Rahman
Analytical Chemistry Division, Department of Chemistry, Aligarh Muslim University, Aligarh U P, India
Pharmazie 59:112-6. 2004..Statistical comparison of the results with the reference method shows excellent agreement and indicates no significant difference in accuracy and precision...
Quantitative analysis of rabeprazole sodium in commercial dosage forms by spectrophotometryNafisur Rahman
Department of Chemistry, Aligarh Muslim University, Aligarh, Uttar Pradesh, India
Chem Pharm Bull (Tokyo) 56:995-1001. 2008..38 and 0.75 microg ml(-1), respectively. Both methods have been applied successfully for the estimation of rabeprazole sodium in commercial dosage forms. The results are compared with the reference UV spectrophotometric method...
Kinetic spectrophotometric determination of famotidine in commercial dosage formsNafisur Rahman
Analytical Research Division, Department of Chemistry, Aligarh Muslim University, Aligarh U P 202002, India
Anal Sci 19:907-11. 2003..The method has been applied to the determination of famotidine in tablet formulations. The obtained results are compared statistically with those given by a reference spectrophotometric method...
Extractive spectrophotometric methods for the determination of nifedipine in pharmaceutical formulations using bromocresol green, bromophenol blue, bromothymol blue and eriochrome black TNafisur Rahman
Department of Chemistry, Analytical Chemistry Division, Aligarh Muslim University, Aligarh 202002, Uttar Pradesh, India
Farmaco 59:47-54. 2004..No interference was observed from common pharmaceutical adjuvants. Statistical comparison of the results with the reference method shows excellent agreement and indicates no significant difference in accuracy and precision...
Kinetic spectrophotometric method for the determination of norfloxacin in pharmaceutical formulationsNafisur Rahman
Department of Chemistry, Aligarh Muslim University, Aligarh, India
Eur J Pharm Biopharm 57:359-67. 2004..Statistical comparison of the results with the reference method shows excellent agreement and indicates no significant difference in accuracy and precision...
Optimized and validated initial-rate method for the determination of perindopril erbumine in tabletsNafisur Rahman
Analytical Research Division, Department of Chemistry, Aligarh Muslim University, India
Chem Pharm Bull (Tokyo) 54:33-6. 2006..Statistical comparison of the results with the Abdellatef's spectrophotometric method shows excellent agreement and indicates no significant difference between the methods compared in terms of accuracy and precision...
Application of oxidants to the spectrophotometric determination of amlodipine besylate in pharmaceutical formulationsNafisur Rahman
Analytical Research Division, Department of Chemistry, Aligarh Muslim University, Aligarh, 202002 UP, India
Farmaco 59:913-9. 2004..The proposed methods were applied successfully to the determination of amlodipine besylate in commercial tablets...
Application of ninhydrin to spectrophotometric determination of famotidine in drug formulationsNafisur Rahman
Department of Chemistry, Analytical Chemistry Division, Aligarh Muslim University, 202 002 Aligarh, India
Farmaco 58:1045-50. 2003..99 x 10(3) l M(-1) cm(-1). The results were validated statistically. The proposed method has been applied to the determination of famotidine in tablets with satisfactory results...
A sensitive kinetic spectrophotometric method for the determination of captopril in bulk and dosage formsNafisur Rahman
Analytical Research Laboratory, Department of Chemistry, Aligarh Muslim University, Aligarh 202002, U P India
Acta Pharm 56:347-57. 2006..The experimental true bias of all samples is lower than +/- 2%. The proposed method has been applied to the determination of captopril in bulk and dosage forms...
Hypothesis testing for the validation of the kinetic spectrophotometric methods for the determination of lansoprazole in bulk and drug formulations via Fe(III) and Zn(II) chelatesNafisur Rahman
Department of Chemistry, Aligarh Muslim University, India
Drug Test Anal 2:137-43. 2010..The inter-day and intra-day precision data showed good accuracy and precision of the proposed procedure for analysis of lansoprazole. The point and interval hypothesis tests indicate that the proposed procedures are not biased...
Spectrophotometric determination of verapamil hydrochloride in drug formulations with chloramine-T as oxidantNafisur Rahman
Analytical Research Division, Department of Chemistry, Aligarh Muslim University, Aligarh 202002, India
Anal Bioanal Chem 374:484-9. 2002..Statistical comparison of the results with those from the reference method reveals excellent agreement and confirms that accuracy and precision are not significantly different...
Application of pi-acceptors to the spectrophotometric determination of lisinopril in commercial dosage formsNafisur Rahman
Department of Chemistry, Analytical Research Laboratory, Aligarh Muslim University, Aligarh, UP 202 002, India
Farmaco 60:605-11. 2005..432x10(4) and 1.192x10(4) l mol-1 cm-1 for TCNQ and pCA methods, respectively. Both the methods have been applied to the determination of lisinopril in pharmaceutical dosage forms. Results of analysis are validated statistically...
New spectrophotometric methods for the determination of nifedipine in pharmaceutical formulationsNafisur Rahman
Department of Chemistry, Aligarh Muslim University, Aligarh, India
Acta Biochim Pol 52:915-22. 2005..No interference was observed from common pharmaceutical adjuvants. The reliability and the performance of the proposed methods are established by point and interval hypothesis tests and through recovery studies...
Validation of simultaneous volumetric and spectrophotometric methods for the determination of captopril in pharmaceutical formulationsNafisur Rahman
Analytical Research Division, Department of Chemistry, Aligarh Muslim University, Aligarh 202 002, UP, India
Farmaco 60:569-74. 2005..Comparison of the means of the proposed procedures with those of reference methods using point and interval hypothesis tests showed no statistically significant difference...
Validated spectrophotometric methods for the determination of amlodipine besylate in drug formulations using 2,3-dichloro 5,6-dicyano 1,4-benzoquinone and ascorbic acidNafisur Rahman
Analytical Chemistry Division, Department of Chemistry, Aligarh Muslim University, Aligarh U P 202 002, India
J Pharm Biomed Anal 31:381-92. 2003..Both the methods were applied successfully for the analysis of amlodipine besylate in dosage forms. Results of analyses were validated statistically and through recovery studies...
Validated kinetic spectrophotometric method for the determination of metoprolol tartrate in pharmaceutical formulationsNafisur Rahman
Department of Chemistry, Aligarh Muslim University, Aligarh 202002 U P, India
Chem Pharm Bull (Tokyo) 53:942-8. 2005..Statistical comparison of the results with the reference method shows excellent agreement and indicates no significant difference in accuracy and precision...
Optimized and validated spectrophotometric method for the determination of uranium(VI) via complexation with meloxicam- Lutfullah
Department of Chemistry, Aligarh Muslim University, Aligarh 202002, Uttar Pradesh, India
J Hazard Mater 155:261-8. 2008..Results of analysis were statistically compared with those obtained by Currah's spectrophotometric method showing acceptable recovery and precision...
Development and validation of spectrofluorimetric method for determination of haloperidol in pharmaceutical dosage formsNafisur Rahman
Department of Chemistry, Aligarh Muslim University, Aligarh, U P, India
Drug Test Anal 2:252-8. 2010..Statistical comparison of the results with the reference method shows excellent agreement and indicates no significant difference between the methods compared in terms of accuracy and precision...
Spectrofluorimetric method for the determination of doxepin hydrochloride in commercial dosage formsNafisur Rahman
Department of Chemistry, Aligarh Muslim University, Aligarh, 202002, Uttar Pradesh, India
AAPS PharmSciTech 10:1381-7. 2009..95 ng ml(-1). The method has been successfully applied to the determination of doxepin hydrochloride in commercial dosage forms. The results are compared with the reference spectrofluorimetric method...
Development and validation of fixed-time method for the determination of isoxsuprine hydrochloride in commercial dosages formsNafisur Rahman
Department of Chemistry, Aligarh Muslim University, UP, India
Drug Test Anal 2:442-6. 2010..Statistical comparison (point and interval hypothesis tests) of the results showed that there is no significant difference between the proposed method and reference method...
